Precision and accuracies fell within acceptable limits (20 % for LLOQ and 15 %) for both intra- and inter-day analyses for all compounds except acetaldehyde which had inter-day variability of ≤25 %. PLoS One 7:e49407. This method was successfully applied for the quantification of ethanol in whole blood samples collected from autopsy cases. Calibration curves that were constructed for ethanol spiked into blank samples followed linear relationships with highly significant (p < 0.001) correlation coefficients (r > 0.999). Beitr Gerichtl Med 36:275–279, Iffland R, Grassnack F (1995) Epidemiologic study of CDT (carbohydrate-deficient transferrin) and other indicators of alcohol problems in high blood alcohol German automobile drivers. We use cookies to help provide and enhance our service and tailor content and ads. https://doi.org/10.1007/s00216-013-6809-1, DOI: https://doi.org/10.1007/s00216-013-6809-1, Over 10 million scientific documents at your fingertips, Not logged in For fish stew cooked for 45 min in a covered pan where the wine was added in cold ingredients, alcohol retention was 30%, whereas for beef bib and hunter rabbit with red wine added to boiling ingredients and then cooked for 1 h in a covered pan the ethanol retention was 5%. J Chromatogr A 1252:23–30, Ashley DL, Bonin MA, Cardinali FL, McCraw JM, Holler JS, Needham LL, Patterson DG Jr (1992) Determining volatile organic compounds in human blood from a large sample population by using purge and trap gas chromatography/mass spectrometry. Quantification of ethanol was successfully performed in fish stew and beef bib by external standard method. A headspace SPME method in combination with GC/MS was used for the extraction, identification, and quantification of ethanol. Int J Toxicol 22:377–380, Whittaker A, Currie AE, Turner MA, Field DJ, Mulla H, Pandya HC (2009) Toxic additives in medication for preterm infants. 2 > 0.99) and the limits of detection were 0.1–0.2 mg/L and lower limits quantification 0.5–1 mg/L. Copyright © 2020 Elsevier B.V. or its licensors or contributors. Copyright © 2010 Elsevier Ltd. All rights reserved. Whereas standard addition method was used for quantification of ethanol in hunter rabbit, marinated grilled steak and industrial products that refer ethanol in the ingredients. J Chromatogr B Anal Technol Biomed Life Sci 773:75–82, Wasfi IA, Al-Awadhi AH, Al-Hatali ZN, Al-Rayami FJ, Al Katheeri NA (2004) Rapid and sensitive static headspace gas chromatography–mass spectrometry method for the analysis of ethanol and abused inhalants in blood. Immediate online access to all issues from 2019. volume 405, pages4139–4147(2013)Cite this article. J Toxicol Clin Toxicol 37:75–81, Hadjiioannou TP, Hadjiioannou SI, Avery J, Malmstadt HV (1976) Automated enzymic determination of ethanol in blood, serum, and urine with a miniature centrifugal analyzer. The work described here was funded by the ESNEE project which is conducted under ERA-NET PRIOMEDCHILD. 1, 1, 1 –Trichloroethane15, Xylene, Trichloroethylene and Dimethylformamide16, Benzene17 and Lead.18, 19 May cause harmful central nervous system effects. Forensic Sci Int 128:115–119, Article  ► Recommendations of intake of meals cooked with alcoholic drinks by pediatric age group and abstinent alcoholics. Il Farmaco 58:541–550, Osterberg RE, See NA (2003) Toxicity of excipients—a food and drug administration perspective. Part of Springer Nature. Ethanol production, purification, and analysis techniques: a review Abstract World ethanol production rose to nearly 13.5 billion gallon in 2006. Ethanol drinking is also suspected of increasing the toxic effect of other chemicals encountered in the laboratory and the workplace by inhibition of their metabolism or excretion14; e.g. Anal Chim Acta 522:163–168, Zuba D, Parczewski A, Reichenbacher M (2002) Optimization of solid-phase microextraction conditions for gas chromatographic determination of ethanol and other volatile compounds in blood. A fibre coated with 75 μm CAR/PDMS film was chosen to extract the ethanol. Baseline levels of acetaldehyde, acetone, methanol and ethanol could be measured in patients before dosing commenced and an increase in levels of some volatiles were observed in several neonates after receiving ethanol-containing medications. Copyright © 2010 Elsevier Ltd. All rights reserved. In this work, we prepared a model MgO–SiO2 catalyst by impregnation of MgO onto an SBA-15 support and used this material to study the reaction kinetics of ethanol dehydrogenation to acetaldehyde. Pediatr Crit Care Med 10:256–259, Crato H, Walther G, Herrmann A (1978) The occurrence of acetone in blood samples forwarded for alcohol content analysis. Coefficients of variation of <7.9% indicated that the technique was reproducible. Dean et al. Forensic Sci Int 161:151–157, Macchia T, Mancinelli R, Gentili S, Lugaresi EC, Raponi A, Taggi F (1995) Ethanol in biological fluids—headspace GC measurement. Tax calculation will be finalised during checkout. Google Scholar, Kugelberg FC, Jones AW (2007) Interpreting results of ethanol analysis in postmortem specimens: a review of the literature. GC-MS analysis of ethanol and other volatile compounds in micro-volume blood samples—quantifying neonatal exposure. (5) reported a method for simultaneous determination of ethanol and ethyl-d5 alcohol in serum using stable isotope GC/MS. ► Potential hazards of intake of meals cooked with alcoholic drinks by ethanol sensible individuals. Med Sci Law 43:241–247, Kristoffersen L, Stormyhr L-E, Smith-Kielland A (2006) Headspace gas chromatographic determination of ethanol: the use of factorial design to study effects of blood storage and headspace conditions on ethanol stability and acetaldehyde formation in whole blood and plasma. Google Scholar, Christophersen AS, Gjerde H, Bjorneboe A, Sakshaug J, Morland J (1990) Screening for drug use among Norwegian drivers suspected of driving under influence of alcohol or drugs. Wasfi et al. Subscription will auto renew annually. Ethanol has been part of alcoholic beverages for long time, but its application has expanded much beyond that during the 20th Century. Department of Chemistry, University of Leicester, Leicester, LE1 7RH, UK, Department of Infection Immunity and Inflammation, University of Leicester, Leicester, LE1 7RH, UK, Neonatal Unit, University Hospitals Leicester, Leicester, LE1 5WW, UK, Division of Perinatal and Developmental Medicine, University of Liverpool, Liverpool, L69 3BX, UK, You can also search for this author in ► Prediction of ethanol content of meals cooked with alcoholic drinks. For fish stew cooked for 45 min in a covered pan where the wine was added in cold ingredients, alcohol retention was 30%, whereas for beef bib and hunter rabbit with red wine added to boiling ingredients and then cooked for 1 h in a covered pan the ethanol retention was 5%. The method used for sample preparation was simple. J Anal Toxicol 19:241–246, Portari GV, Marchini JS, Jordao AA (2008) Validation of a manual headspace gas chromatography method for determining volatile compounds in biological fluids. ScienceDirect ® is a registered trademark of Elsevier B.V. ScienceDirect ® is a registered trademark of Elsevier B.V. Headspace SPME–GC/MS evaluation of ethanol retention in cooked meals containing alcoholic drinks. ► Prediction of ethanol content of meals cooked with alcoholic drinks. Analytical and Bioanalytical Chemistry The use of dealcoholised wine evaluated as a tasty alternative to the above mentioned groups. Both liquids require the addition of some other chemical or contamination of some sort. ScienceDirect ® is a registered trademark of Elsevier B.V. ScienceDirect ® is a registered trademark of Elsevier B.V. Headspace SPME–GC/MS evaluation of ethanol retention in cooked meals containing alcoholic drinks. Google Scholar, Zuba D, Piekoszewski W, Pach J, Winnik L, Parczewski A (2002) Concentration of ethanol and other volatile compounds in the blood of acutely poisoned alcoholics. Infant 7:196–199, Alonso M, Castellanos M, Besalu E, Sanchez JM (2012) A headspace needle-trap method for the analysis of volatile organic compounds in whole blood. We use cookies to help provide and enhance our service and tailor content and ads. ► Recommendations of intake of meals cooked with alcoholic drinks by pediatric age group and abstinent alcoholics. The method was applied to analyse blood samples from neonatal patients receiving courses of ethanol excipient containing medications. The limits of quantification were registered at levels of parts per million. Arch Dis Child Fetal Neonatal Ed 94:F236–F240, Shehab N, Lewis CL, Streetman DD, Donn SM (2009) Exposure to the pharmaceutical excipients benzyl alcohol and propylene glycol among critically ill neonates. PubMed Google Scholar. https://doi.org/10.1016/j.foodchem.2010.11.117.

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